Product Information

2,3-Difluorophenol CAS NO. 6418-38-8 has a molecular formula of C6H4F2O and a molecular weight of 130.09. It is a white solid crystal. The boiling point is 54°C. The melting point is 39°C-41°C. The flash point is 56°C. It is highly flammable, and is harmful by inhalation, skin contact and swallow. It will cause burns and irritate eyes, respiratory system and skin.

Resolve Resolution of 2,3-Difluorophenol CAS NO. 6418-38-8

Using 2,3,4-trifluoroaniline as raw material, through two steps of diazotization and hydrolysis, and then adopting appropriate treatment methods to obtain 2,3-difluorophenol, the synthesis conditions were studied. The experimental results show that: when diazotization The reaction temperature of preparing trifluoroaniline sulfate and adding sodium nitrite dropwise should be controlled at about 55 ℃ and 15℃, respectively; the optimal hydrolysis temperature of diazonium salt is 50-55 ℃, and the mass fraction of 0.5 is added when reacting with hypophosphorous acid. % catalyst, the highest yield can be obtained. The obtained product has a melting point of 33.8~35.6 °C, a purity of ≥99.6%, and a yield of ≥65%.

Specifications:

CAS NO. 6418-38-8

Appearance: white crystalline low melting mass
Purity: 99%min

Boiling point: 54ºC (25 mmHg)

Melting point: 33-39ºC

Packing: 25kg or 50kg net plastic drum

Storage Condition: Flammables area

Store in a cool, dry place. Store in a tightly closed container. Stable under normal temperatures and pressures.

Safety Info: